This time, Rafael Nadal could not summon the third-set magic he needed.
Coming off an epic three-hour duel Wednesday in his first match since the French Open final, Nadal fell to Lloyd Harris 6-4 1-6 6-4 on Thursday at the Citi Open.
After a short-lived maiden appearance at the Washington, D.C. tournament, the Spaniard will look ahead to Toronto and Cincinnati as he continues his preparations for the U.S. Open.
Harris, meanwhile, heads to a quarter-final matchup against veteran Kei Nishikori after recording the biggest win of his career.
Facing Nadal for the first time, the 24-year-old South African slammed 16 aces Thursday and saved four of six break points.
The 20-time grand slam winner, who battled a foot injury to outlast Jack Sock in his first match, did not have enough to answer the world number 50 on Thursday.
In addition to the top-seeded Nadal's defeat, second seed Felix Auger-Aliassime also went down Thursday, falling 6-3 6-4 to American wild card Jenson Brooksby.
With their exits, the tournament is now without its top four seeds.
That leaves fifth seed Jannik Sinner as the top player remaining after he defeated Sebastian Korda 7-6 (7-3) 7-6 (7-3).
Nishikori advanced by downing seventh seed Cameron Norrie 3-6 6-3 6-3, while John Millman knocked out eighth seed Reilly Opelka 6-3 7-6 (7-4).
Among unseeded players, Denis Kudla defeated the red-hot Brandon Nakashima 3-6 7-6 (7-3) 6-4, while Steve Johnston eased past Ricardas Berankis 6-2 6-1 and Mackenzie McDonald beat Illya Ivashka 6-4 6-4.
In addition to Harris-Nishikori, Kudla will face McDonald in the other quarter-final in the top half of the draw, while Sinner meets Johnson and Millman takes on Brooksby in the bottom half.
Dominant Djokovic breezes past Cobolli in Shanghai
Novak Djokovic's hopes of claiming a 100th tour-level title are still alive after cruising past Flavio Cobolli at the Shanghai Masters.
After being pushed all the way by Alex Michelsen in his opener, the Serb looked much more comfortable as he triumphed 6-1 6-2 in the third round in just 64 minutes.
He got an early break to take control in the first set, racing into a 3-0 lead before Cobolli got on the board, but another three-game winning streak for Djokovic gave him the first set.
The Italian started the second set brighter, going toe to toe as they traded blows in the opening games.
However, Djokovic soon regained control, and though Cobolli managed to save five of the nine break points he faced during the match, he could do little as the 37-year-old won the final five games to progress.
Djokovic will now face Roman Safiullin in the fourth round.
Data Debrief: Cruise control
Since the format's inception in 1990, Djokovic (82.02%, 406-89) has surpassed Rafael Nadal (82.00%, 410-90) for the highest winning percentage of any player at ATP Masters 1000 events - minimum 10 matches.
And he did so in dominant fashion. He struck 11 winners in the first set (19 overall), and won 20 of his 24 first-serve points throughout the game (83%).
Gauff reassured she is moving in 'right direction' after China Open win
Coco Gauff believes she has proven to herself that she is going in the "right direction" after winning the China Open in Beijing.
Gauff triumphed 6-1 6-3 in Sunday's final, beating Karolina Muchova in just 76 minutes to claim her second title of 2024, after winning the Auckland Open in January.
She is also now the first player to win each of her first seven WTA hard-court finals in the Open Era.
However, after winning the Cincinnati Open and her maiden grand slam at the US Open last year, Gauff struggled at the start of the hard court swing this time around.
After an early exit at the Paris Olympics, she only won once across at Toronto and Cincinnati before seeing her US Open title defence ended in the last 16 by Emma Navarro.
"Everybody can do everything in practice," Gauff told WTA Insider. "This time, when the pressure is on the line, I was just trying to force myself to do things I was uncomfortable with.
"So yeah, I think the result is now reassurance that I am in the right direction.
"A lot of times people forget that I'm still in the developmental phase of my career and nothing is going to be great.
"Most of the people doing well are 25 and older in the top 10, maybe with the exception of Iga [Swiatek]. We have a long way to go, and I still have a lot that I need to work on, and I'm proud of myself thus far.
"I didn't have a complete game at 15, and I don't have one right now, but I've been on tour playing every week almost, trying to be better. I'm just super proud of that."
Gauff will be in action next at the Wuhan Open, making her first appearance at the tournament.
Osaka pulls out of home Japan Open through injury
Naomi Osaka will not play at her home Japan Open next week due to a back injury, organisers confirmed on Monday.
The 26-year-old was forced to retire during the last 16 against eventual champion Coco Gauff at the China Open in Beijing last week because of the same injury.
Osaka was on a three-match winning streak before her meeting with Gauff, having also registered her first comeback victory in two years earlier in the tournament when she beat Yulia Putintseva in the second round.
However, the four-time grand slam winner has not recovered in time and will not be able to play on home soil when the tournament starts on October 14.
"Due to injury, Naomi Osaka has decided to withdraw from the tournament," the Japan Tennis Association said in a statement.
Osaka is still scheduled to play in the Pan Pacific Open Tennis Tournament 2024 in Tokyo, which begins on October 21.
Her last appearance in her home country was at that tournament in 2022, when she withdrew in the second-round match with abdominal pains.
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