Cameron Norrie suffered an agonising end to his Australian Open run as he was pipped in a fifth-set tie-break by Alexander Zverev after a terrific fourth-round tussle.
The British number one broke new ground with a brilliant attacking display to defeat Casper Ruud on Saturday and again showed the new dimensions he has added to his game to push the sixth seed all the way.
Norrie, who had not won a set in their four previous meetings, twice came from behind to force a decider but it is Zverev who moves through to the quarter-finals after a 7-5 3-6 6-3 4-6 7-6 (10/3) victory.
Norrie will leave Australia, though, knowing that he can mix it with the best players in the world on the biggest stage and with confidence fully restored after a shaky second half of last season.
The match was briefly interrupted in the third set by a protester, who threw ‘Free Palestine’ flyers onto the court from the front row of Margaret Court Arena before being forcibly escorted away by two spectators.
The scenes were reminiscent of Wimbledon last summer, when Just Stop Oil protesters threw jigsaw pieces and confetti onto the court during two matches, although the leaflets were swiftly cleared here and play quickly resumed.
Norrie’s tactics against Ruud came as no surprise to Zverev, who spent the off-season practising with the British number one in Monte-Carlo.
There were few rallies of any kind in the first set, with serve dominating until Norrie, who was trying to beat a top-10 opponent at a slam for the first time, was broken at 5-5.
Zverev immediately came under pressure on serve for the first time but saved a break point with a forehand onto the line, and looked to have taken control of the contest when he broke again to lead 3-2 in the second.
However, Norrie played what must be one of the best returning games of his career to hit straight back, finishing it off with a zinging backhand cross-court winner.
And Norrie was not finished there, the 28-year-old showing his new-found aggression and willingness to mix up his tactics to pile more pressure on Zverev in his next service game.
The German saved two break points but then mis-hit a forehand on the third and suddenly Norrie was serving for the set.
It was far from straightforward for the 19th seed but he saved four break points before taking it, fortuitously, when a forehand hit the top of the net and dropped over.
A poor service game at 1-2 in the third set was enough for Zverev to take it and though Norrie pushed hard at the beginning of the fourth set, Zverev managed to save two break points in the second game.
However, the Olympic champion was powerless to stop Norrie forcing a decider, the 28-year-old creating two set points at 4-5 and taking the first with a delicate half-volley.
Norrie was managing to bully Zverev, one of the most powerful players on tour, at times from the baseline, while his drop shots and short angled slices kept the German guessing.
They exchanged breaks of serve at the start of the fifth set while Norrie survived a tense game at 3-3, saving three more break points.
Both men managed to hold serve through to a first-to-10-points tie-break but there Norrie’s resistance ran out, with Zverev clinching the win after four hours and five minutes to end British interest in the singles.
Sinner avoids O'Connell upset at US Open
Jannik Sinner beat Australia's Christopher O'Connell in straight sets to reach the fourth round of the US Open on Saturday, avoiding a similar fate to Carlos Alcaraz and Novak Djokovic.
The men's draw at Flushing Meadows has been blown wide open by early exits for Alcaraz and Djokovic, but the top seed remains in the hunt after a composed performance.
He reached the fourth round for a fourth consecutive year with a routine 6-1 6-4 6-2 victory, setting the tone with several huge groundstrokes in the opening set.
O'Connell never looked likely to fight back as Sinner smashed 46 winners in a ruthless performance, wrapping up his win in one hour and 56 minutes.
The Australian Open champion will face either Tommy Paul or Gabriel Diallo for a place in the last eight, and he was relieved to survive an opening week full of surprises.
"Everything can happen in this sport, so I try to stay on my side of the net and I'm trying to take the tournament day by day," Sinner said in his on-court interview after the win.
"Each opponent is a very tough challenge and [I am] also enjoying every moment on the court. There have been already a couple of upsets, so let's see what's coming.
"But I'm very happy to still be here and hopefully I can play as many matches as possible. But as I said, we go day by day and then we'll see how it goes."
Data Debrief: Sinner heating up
Sinner lost his first set of the tournament to Mackenzie McDonald but has been largely untouchable since then.
He has only lost 18 games across his last nine sets of tennis, an average of two per set.
The Italian's winning streak now stands at seven straight matches, meanwhile, following his triumphant Cincinnati Open run.
US Open: Sabalenka overcomes first set scare to progress in late start
Aryna Sabalenka came from a set down to keep her US Open dream alive as she beat Ekaterina Alexandrova in the early hours at Flushing Meadows.
Sabalenka emerged on court at the Arthur Ashe Stadium at seven minutes past midnight following Novak Djokovic's shock exit from the tournament, and consecutive upsets looked to be on the cards.
However, the Belarusian responded from a disappointing opening set as she looks to avenge her defeat in the showpiece match against Coco Gauff a year ago.
The world number two set up a meeting with Belgium's Elise Mertens as she emerged a 2-6 6-1 6-2 victor in one hour and 40 minutes in New York.
"I don't know what I did, I was just trying to stay low, put as many balls as I can back on that side," Sabalenka said.
"She played incredible tennis in the first set. It was really tough to change it."
"I'm really happy I was able to turn around this match and get this really difficult win. Thanks so much for staying that late."
Data Debrief: Sabalenka survives late, late show
Sabalenka's encounter with Alexandrova was the latest starting match at the US Open, beating Gabriela Sabatini and Beverley Bowes' meeting in 1987 that started at midnight.
The Belarusian, however, will be hoping for a much improved performance in the next round, having produced 27 unforced errors throughout the contest and serving four double faults.
US Open: Djokovic played 'worst tennis ever' in Popyrin loss
Defending US Open champion Novak Djokovic suffered a shock exit at Flushing Meadows as he lost in four sets to Alexei Popyrin.
Djokovic arrived at the tournament with confidence following his gold medal triumph at the Paris Olympics, and was tipped to lift a record-extending 25th grand slam title.
However, the Serbian's hopes of a fifth success in New York were dashed as he followed fellow favourite Carlos Alcaraz out of the competition in the third round.
Popyrin emerged victorious in three hours and 18 minutes, prevailing 6-4 6-4 2-6 6-4 to confirm Djokovic's earliest exit from the tournament in 18 years.
"I have played some of the worst tennis I have ever played," Djokovic said.
"Honestly, the way I felt and the way I played from the beginning of this tournament, third round is a success."
"I tried my best, I didn't have any physical issues. I just felt out of gas, and you could see that. From the first match, I just didn't find myself on this court.
"Life moves on. I'll try to recalibrate and look forward to what's next."
Data Debrief: Another one bites the dust
Djokovic was far from his clinical best, serving a career-high 14 double faults in a grand slam match and committing 49 unforced errors.
The Serbian will also end the year without winning a grand slam title, the first time he has done so since 2017.
But the day belonged to Popyrin, saving 12 of the 16 break points he faced against the world number two, finding particular success with his forehand as 31 of his 49 winners came from that shot.
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