Justin Rose mounted a back-nine recovery to finish his second round with a two-shot lead over Jordan Spieth and Marc Leishman.
Rose shot a sublime opening round of 65 at Augusta, but relinquished his four-shot advantage on Friday before returning to the top of the leaderboard with three birdies in his space of four holes.
The Englishman was the man to catch on seven under when he signed for a level-par 72, rallying after bogeying four of the first seven holes in his second round.
Gains at the 13th, 14th and 16th holes gave Rose momentum heading into the weekend as he bids to don the green jacket for the first time.
The in-form Spieth surged into a share of second place with Australian Leishman by carding a four-under 68, with birdies proving easier to come by for the field than on the opening day.
Three-time major champion Spieth, on a high after ending a title drought stretching back to 2017 at the Texas Open last weekend, made four of his five birdies after the turn and only dropped one shot at the 12th.
Leishman also made a significant move, setting the tone by starting with three birdies in row and going on to shoot a five-under 67.
Scintillating six-under rounds of 66 from Bernd Wiesberger and Tony Finau put them just three shots adrift of Rose along with Justin Thomas, who shot a 67.
Will Zalatoris, Brian Harman and Si Woo Kim were also well poised on four under, with their rounds still in progress. Defending champion Dustin Johnson had work to do back on three over through 10.
Bryson DeChambeau responded to a poor opening round with a 67 of his own to sit at one over, while Brooks Koepka (+5) and Rory McIlroy (+6) were facing a battle to make the cut 10 and eight holes into their rounds respectively.
Lee Westwood was a couple of shots below the projected cut mark on five over midway through his round.
'The game is testing me' – More agony for McIlroy as Horschel wins BMW PGA Championship
Rory McIlroy admitted golf is "testing" him more than usual after enduring yet another near miss at the BMW PGA Championship, losing to Billy Horschel in a play-off.
McIlroy, Horschel and Thriston Lawrence were forced into a three-way play-off after they all finished 20-under through four rounds at Wentworth.
Lawrence carded a final round of 65 to close a two-shot gap to McIlroy and Horschel, but the South African bogeyed the first play-off hole to put himself out of contention.
Horschel then wrapped up his second triumph at Wentworth with an eagle on the second, having previously triumphed at the event in 2021.
McIlroy has endured a frustrating year, missing two close-range putts when in pole position to win the US Open in June, then slipping again on the final round to finish second at last week's Irish Open.
Speaking after Sunday's play-off, the Northern Irishman said: "Last week was a tough one but I left there with my head held high with the way I played the last hole, trying to make three.
"Two weeks in a row I've played well. Just not quite well enough. The game is testing me a little more than it has done in the past, but that's fine.
"It could have been a different year but the nice thing is there's next year and the year after and the year after and the year after.
"If you think of my career as a 30-year journey, it's only one year in a 30-year journey, and hopefully the other 29 are a little more productive or a little bit better."
Horschel, meanwhile, admitted the struggles of the four-time major winner, a close friend of his, put a slight dampener on his victory.
"I'm thrilled and excited for the way I played," Horschel said.
"At the same time I'm a little disappointed – Rory is a great friend of mine and he's a generational talent. I know how close he's been this year so I feel for him.
"I needed a bit of luck. There was a lot of luck on my side to get this victory today."
McIlroy pleased with 'solid' round as he chases Manassero at Wentworth
Rory McIlroy was pleased with a 'solid' bogey-free round of 66 as he sits joint-second on 15 under par, three shots off leader Matteo Manassero, ahead of the final day of the BMW PGA Championship.
McIlroy carded a six-under round with four birdies and one eagle on the fourth, only bettered by leader Manassero's 63 and Billy Horschel's 65, which included a run of seven straight birdies and put him in a tie for second alongside the Northern Irishman.
The 35-year-old, who won the event in 2014, was happy enough with his third round, despite finding the water on 18 and scrambling a par on the scoreable final hole.
He said to Sky Sports: "I had a few chances that I let slip there on the back nine, but I got going out there on moving day, shooting six under par, trying to keep up with Matteo.
"It was another solid day, my lowest score of the week and no bogeys. I know I'm going to need another low one tomorrow to try to catch him.
"I love it here. It would be amazing to get my name on the trophy again."
Manassero, who also tasted success at Wentworth in 2013, was delighted with his round, coming towards the end of a season in which he has returned from the wilderness to play some of his very best golf.
"I have to be honest, one of the best rounds I've ever played," the Italian said afterwards.
"Thinking of the difficult years, to be standing here right now in the lead - it feels amazing."
"My perspective has changed. I'm going to go out and enjoy tomorrow."
Spieth expecting to be tournament ready for 2025 PGA season
Jordan Spieth is expecting to return to action for the 2025 PGA Tour season after undergoing successful wrist surgery last month.
Spieth, who last competed at the FedEx St. Jude Classic at TPC Southwind, failed to find his best form during the recent campaign out on the course.
The former world number one started the season strong, finishing third in The Sentry and then, a few weeks later, tied for sixth in the WM Phoenix Open
But the American missed the final two playoffs in the BMW Championship and Tour Championship, while also missing seven cuts, one of which included the Masters.
Spieth was seen sporting a cast on his first appearance since the surgery and was able to reveal the timeline for his return to action.
"I think that by 2025, by Jan. 1, it's my goal to be tournament-ready," Spieth told Golfweek in a Q&A published on Monday.
"And for me, that would be not just going out and seeing how it feels, you know, but expecting to play at my ceiling."
Spieth has three major wins and 13 overall victories on the PGA Tour but has not emerged victorious since the RBC Heritage in April 2022.
The American did not earn entry into the 2025 season-opening tournament. However, he is able to play in the Sony Open in Hawaii at the start of January.
While the 31-year-old's main reason for surgery was to see him return to form, he also detailed the personal reasons for his decision to go under the knife.
"I would say the number one reason why I ended up getting it done was because it affects my way of life at home," Spieth said.
"Like when it would dislocate and I couldn't get it back in, it would happen when I'm getting my daughter out of the bath, I'm putting a sweatshirt on or it just so random that it was like, I didn't want it to continue, and it happened more and more.
"And it wasn't going to heal itself based on a number of different docs and scans and whatever. So it's just inevitable."
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