Girona’s hopes of reducing the deficit to LaLiga leaders Real Madrid were dashed by a 3-2 defeat to Athletic Bilbao at the San Mames Stadium.
The surprise early-season pace-setters had only themselves to blame after two defensive blunders handed the home side the chance to stretch their unbeaten league run to four games.
The visitors, who remain six points behind Real Madrid, got off to a nightmare start when a rash cross-field ball by Aleix Garcia fell to Alejandro Berenguer, whose cool strike gave Bilbao the lead with just over two minutes on the clock.
Girona hit back to level when Viktor Tsygankov turned the ball home from close range four minutes after the interval, but moments later Berenguer grabbed his second after a mistake from Miguel Gutierrez on the right flank.
Inaki Williams made up for a series of missed early opportunities when he fired home from the centre of the box on the hour mark to move the home side to the brink of victory.
But Girona showed some of the fight that has served them so well this season as they reduced the deficit to 3-2 on 75 minutes when Eric Garcia met a cross into the box.
And the visitors came agonisingly close to pulling level five minutes into injury time when Savio failed with his initial effort only for the ball to fall to team-mate Jhon Solis, whose shot on the rebound was brilliantly blocked on the line by Bilbao defender Daniel Vivian.
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Celta Vigo 2-2 Barcelona: Stunning late show denies 10-man Blaugrana
Celta Vigo scored two goals in two minutes late on to earn an entertaining 2-2 draw with Barcelona in LaLiga at the Estadio Abanca-Balaidos.
League leaders Barca appeared to be cruising towards victory when they opened up a two-goal lead thanks to captain Raphinha and leading goalscorer Robert Lewandowski.
Raphinha cut inside before tucking home for the opener 15 minutes in, then Lewandowski got his 15th league goal of the season with a simple finish in the 61st minute.
However, the script changed when Blaugrana midfielder Marc Casado was sent off after receiving his second yellow card in the 82nd minute.
With Barca down to 10 men, the home side piled on the pressure and it told in the 84th minute, substitute Alfonso Gonzalez converting following an error from Jules Kounde.
The comeback was complete two minutes later, with Hugo Alvarez drilling past Inaki Pena to deny Flick's visitors victory.
Despite the result, Barca top LaLiga with 34 points, five ahead of Atletico Madrid in second and seven ahead of third-placed Real Madrid, who have two games in hand.
Data Debrief: Blaugrana finally held
Going into Saturday's game, Barcelona had gone 24 matches without a draw in LaLiga, winning 20 and losing four.
When they entered the final six minutes with a two-goal advantage, it appeared certain they would match their longest streak without a draw in the competition's history, recorded between February and October 2017 (25 games, 23 wins and two draws).
However, Hansi Flick's side were stunned at the death as they dropped points for a second game in succession following a 1-0 loss at Real Sociedad prior to the international break.
Girona 4-1 Espanyol: Miovski bags double as hosts ride on first-half blitz
Bojan Miovski scored twice as Girona thrashed Espanyol 4-1 in LaLiga at Estadi Municipal de Montilivi on Saturday.
Bryan Gil and Ladislav Krejci were also on the scoresheet as the home side raced to a 4-0 lead inside the first half hour, with Javi Puado scoring the visiting side's only goal after the break.
After the match was halted because of a fan being taken ill in the crowd, Gil opened the scoring when he unleashed a stunning long-range strike into the bottom corner with four minutes on the clock.
Gil was behind the second goal for Michel's side too, as he capitalised on a defensive error and crossed to Miovski, who made it 2-0 in the 16th minute before the pair combined again for a third five minutes later.
Donny van de Beek's header from Yaser Asprilla's corner was pushed in by Krejci for Girona's fourth in the 27th minute.
Espanyol got a consolation goal 10 minutes into the second half when Puado hit a long-range strike that found the back of Paulo Gazzaniga's net.
Girona, last season's surprise package, climbed to fifth in LaLiga with 21 points, while Espanyol are 19th and in the relegation zone with 10 points.
'I love where I am,' says Simeone after 700th game in charge of Atletico
Diego Simeone said he is "calm and at peace" at Atletico Madrid after his side edged Deportivo Alaves 2-1 in LaLiga in his 700th game in charge of the club.
Atletico went behind through a Jon Guridi penalty in the seventh minute, but Antoine Griezmann drew them level from the spot in the 76th minute.
The winner came via Alexander Sorloth in the 86th minute as Atletico moved four points behind leaders Barcelona.
Simeone, who has been in charge of Atletico since 2011, is the first coach to manage 700 matches with the same LaLiga club.
"I live in the present, we are having a good time, the boys are working very responsibly," Simeone told DAZN.
"I am calm and at peace. I love where I am and that's it."
He managed Atletico to LaLiga title triumphs in 2014 and 2021 and also helped Los Rojiblancos win two Europa League titles in 2012 and 2018.
The game against Alaves was Simeone's 492nd LaLiga match in charge, and the Argentine has also managed the third-most games with a single club in the Champions League (109), after Alex Ferguson with Manchester United and Arsene Wenger at Arsenal.
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